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- Title
Thermal analysis of anhydrous and hydrated Cholesterol.
- Authors
Kaloustian, J.; Pauli, A.-M.; de Ia Porte, P. Lechene; Lafont, H.; Portugal, H.
- Abstract
Cholesterol constitutes the major component of most gallstones. It was identified and determined, in gallstones, issued from eleven patients, by thermal analysis: differential scanning calorimetry (DSC), with the use of the melting temperature and enthalpy, thermogravimetry (TG), with the mass loss of water. Anhydrous cholesterol (ChA) was characterized by two endothermic peaks (polymorphic, melting) and cholesterol monohydrate (ChH) by two endothermic peaks (dehydration, melting), too. ChA needle and ChH plate crystals were observed under polarizing light microscopy. The numerous stones obtained from nine patients were cholesterol stones: the ChA was higher 45 and lower 96%. ChH was present in stones of three patients.
- Subjects
THERMAL analysis; CHOLESTEROL; GALLSTONES; THERMOGRAVIMETRY; GRAVIMETRIC analysis; CRYSTALS
- Publication
Journal of Thermal Analysis & Calorimetry, 2003, Vol 71, Issue 2, p341
- ISSN
1388-6150
- Publication type
Article
- DOI
10.1023/A:1022818902212