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- Title
Front Cover: One‐pot, Gram‐Scale Synthesis of Calix[5]‐ and Calix[6]furan: Derivatization for Polyketone‐ and Isopyrazole‐based Macrocycles with Conformational Analysis (Asian J. Org. Chem. 5/2024).
- Authors
Yoneda, Tomoki; Sano, Taichi; Pati, Narendra Nath; Ide, Yuki; Inokuma, Yasuhide
- Abstract
This article, published in the Asian Journal of Organic Chemistry, discusses the gram-scale synthesis of calix[n]furans (n = 4, 5, and 6) using size-selective precipitation protocols. The calix[n]furans were then converted to cyclic polyketones and ethylene-bridged cyclic isopyrazoles. The solid-state conformations of these macrocycles were determined through single crystal X-ray diffraction analysis. The study found that the cyclic isopyrazoles formed well-defined cavities with different shapes depending on the value of n. The article provides more details on this research.
- Subjects
DERIVATIZATION; CONFORMATIONAL analysis; HOST-guest chemistry; FURAN derivatives; SINGLE crystals; POLYKETONES
- Publication
Asian Journal of Organic Chemistry, 2024, Vol 13, Issue 5, p1
- ISSN
2193-5807
- Publication type
Article
- DOI
10.1002/ajoc.202480501