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- Title
New Synthesis of Tetrahydroisoquinolines.
- Authors
Dyachenko, I. V.; Dyachenko, V. D.; Dorovatovskii, P. V.; Khrustalev, V. N.; Nenajdenko, V. G.
- Abstract
The reaction of cyclohexylidenecyanothioacetamide with N,N-dimethylformamide dimethyl acetal was studied. This transformation, depending on the reaction conditions, leads to different results: when the starting reagents are refluxed without a solvent, 3-(methylsulfanyl)-5,6,7,8-tetrahydroisoquinoline-4-carbonitrile is formed, and refluxing in benzene leads to 2-cyano-3-(dimethylamino)prop-2-enethioamide. The structure of these products was studied by XRD analysts.
- Subjects
TETRAHYDROISOQUINOLINES; ETHANES; BENZENE; SOLVENTS
- Publication
Russian Journal of Organic Chemistry, 2022, Vol 58, Issue 5, p657
- ISSN
1070-4280
- Publication type
Article
- DOI
10.1134/S1070428022050037