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- Title
Preparation, Spectroscopy, Antimicrobial Assay, and X-Ray Structure of Dimethyl bis-(4-methylpiperidine dithiocarbamato-S,S')-tin(IV).
- Authors
Zia-ur-Rehman; Shahzadi, Saira; Ali, Saqib; Guo-Xin Jin
- Abstract
Dimethyl bis(4-methylpiperidine dithiocarbamato-S,S′)-tin(IV) was synthesized and characterized by elemental analysis, IR and mass spectrometry, multinuclear NMR (¹H- and 13C-NMR), and X-ray single crystal analysis. IR data showed that the ligand acts as a bidentate in the solid state. X-ray data showed the unsymmetrical nature of the ligand towards coordination to tin. It crystallized in the monoclinic P21/n space group. Its geometry is distorted octahedral. Antimicrobial activity data shows that the complex exhibits significantly more activity than the free ligand.
- Subjects
DITHIOCARBAMATES; CARBAMATES; NUCLEAR magnetic resonance; X-rays; ELECTRON spectroscopy
- Publication
Turkish Journal of Chemistry, 2007, Vol 31, Issue 4, p435
- ISSN
1300-0527
- Publication type
Article