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- Title
Suzuki–Miyaura reactions promoted by a PdCl2/sulfonate-tagged phenanthroline precatalyst in water.
- Authors
Li, Qi; Zhang, Li ‐ Ming; Bao, Jia ‐ Jing; Li, Hong ‐ Xi; Xie, Jing ‐ Bo; Lang, Jian ‐ Ping
- Abstract
This work reports of arylboronic acid with aryl halide or aryl dibromide mediated by PdCl2 (0.05 mol%) and sodium 4-(1H-imidazo[4,5-f][1,10]phenanthrolin-1-yl)butane-1-sulfonate (0.05 mol%) at 100 °C in water. The corresponding products were obtained in good to excellent yields. The catalytic system was recovered from the organic products by extraction with ether and the residual aqueous catalyst phase showed high activity after reuse of at least four cycles. Copyright © 2014 John Wiley & Sons, Ltd.
- Subjects
SUZUKI reaction; PHENANTHROLINE; HETEROCYCLIC compounds; BORONIC acids; ARYL halides
- Publication
Applied Organometallic Chemistry, 2014, Vol 28, Issue 12, p861
- ISSN
0268-2605
- Publication type
Article
- DOI
10.1002/aoc.3227