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- Title
Biochemistry, synthesis and identification of (four, five, six and seven) membered heterocyclic derivatives from 4-nitro-5-methylimidazole.
- Authors
Kmal, Rafid Kais; Behget, Shaimaa Adnan
- Abstract
This work included biochemistry and synthesis new azo compound (1-(4-((5-methyl-4-nitro-4, 5- dihydro-1H-imidazol-2-yl) diazenyl) phenyl) ethan-1-one) by reaction 4-nitro-5-methylimidazole with 4-aminoacetophenone in acid medium, then react with 4-aminoantipyrine to get Schiff base derivative. React with (chloroacetylchloride, thioglycolic acid, glycine, alanine, sodium azide, and phthalic anhydride, maleic anhydride) to give (ß-lactam, thiazolidine, imidazolidine, tetrazole, oxazepine) derivatives. The new synthesized compounds have been identified by their melting points, H-NMR, C-NMR and FT-IR spectra.
- Subjects
AZO compound synthesis; HETEROCYCLIC compounds; IMIDAZOLES; BIOCHEMISTRY; SCHIFF base derivatives; THIAZOLIDINEDIONES
- Publication
EurAsian Journal of Biosciences, 2018, Vol 12, Issue 2, p457
- ISSN
1307-9867
- Publication type
Article