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- Title
Crystal structure of the addition compound of N,N′-bi(2-pyridylmethyl)-oxamide and complex of manganese with 1,10-phenanthroline.
- Authors
Liu, Bin; Wang, Hong-Mei; Yan, Shi-Ping; Liao, Dai-Zheng; Jiang, Zong-Hui; Huang, Xiao-Ying; Wang, Geng-Lin
- Abstract
The structure of the addition compound, Mn(phen)3(PMoxdH2)(ClO4)2 was established by X-ray crystallography, where PMoxdH2 is N,N′-bi(2-pyridylmethyl)-oxamide. Six nitrogen atoms of the three 1,10-phenanthroline bind to the manganese ion and the oxygen atom of PMoxdH2 is uncoordinated. The addition compound crystallizes in the monoclinic space group C2/ c, with lattice parameters a = 23.780(6), b = 11.948(5), c = 18.466(6) Å, β = 117.38(3)°, V = 4659(3) Å3, and Z = 4.
- Publication
Journal of Chemical Crystallography, 1999, Vol 29, Issue 5, p623
- ISSN
1074-1542
- Publication type
Article
- DOI
10.1023/A:1009565306738